Columbium versus Niobium

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Volumetric determination of columbium.

The quantitative determination of columbium based on reduction by amalgamated zin c and reox idation with potassium permanganate has, in general, produced results that lack both accuracy and precision. A study of t he various factors involved indicates that essential conditions requ ire adequate duration of reduction in t he presence of an excess of zinc and a proper concentration of both acid ...

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ژورنال

عنوان ژورنال: Nature

سال: 1914

ISSN: 0028-0836,1476-4687

DOI: 10.1038/092528b0